LeHavreV1, France, Analysis, bibRecord, 001102

Facile access to 6‐substituted 1,4,5,7‐tetrahydropyrrolo[3,4‐b]‐pyridines via hantzsch type dimethyl 4‐aryl‐2‐formyl‐6‐methyl‐1,4‐dihydropyridine‐3,5‐dicarboxylates

Identifieur interne : 001102 ( France/Analysis ); précédent : 001101; suivant : 001103

Facile access to 6‐substituted 1,4,5,7‐tetrahydropyrrolo[3,4‐b]‐pyridines via hantzsch type dimethyl 4‐aryl‐2‐formyl‐6‐methyl‐1,4‐dihydropyridine‐3,5‐dicarboxylates

Auteurs : Milostav Chudík [Slovaquie] ; Štefan Marchalín [Slovaquie] ; Peter Knesl [Slovaquie] ; Adam Daich [France] ; Bernard Decroix [France]

Source :

Journal of Heterocyclic Chemistry [ 0022-152X ] ; 2000-11.

RBID : ISTEX:6E2FA2D4C888EFDAEF3F23A4DEC972A4156754B0

Abstract

Efficient assembly of 6‐substituted 4‐aryl‐5‐oxo‐1,4,5,7‐tetrahydropyrrolo[3,4‐b]pyridines (7a‐f) is described according to a Hantzsch type reaction from formyl‐ester 4 by imination, borohydride reduction and intramolecular thermal amino‐ester cyclization. The starting compound 4 was prepared in three steps from the readily available formyl derivative 1, methyl 4,4‐dimethoxy‐3‐oxobutanoate and methyl 3‐aminocrotonate.

Url:

https://api.istex.fr/document/6E2FA2D4C888EFDAEF3F23A4DEC972A4156754B0/fulltext/pdf

DOI: 10.1002/jhet.5570370623

Affiliations:

Links toward previous steps (curation, corpus...)

to stream Istex, to step Corpus: 000138
to stream Istex, to step Curation: 000138
to stream Istex, to step Checkpoint: 000998
to stream Main, to step Merge: 001A07
to stream Main, to step Curation: 001960
to stream Main, to step Exploration: 001960
to stream France, to step Extraction: 001102

Links to Exploration step

ISTEX:6E2FA2D4C888EFDAEF3F23A4DEC972A4156754B0

Le document en format XML

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<author><name sortKey="Chudik, Milostav" sort="Chudik, Milostav" uniqKey="Chudik M" first="Milostav" last="Chudík">Milostav Chudík</name>
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<front><div type="abstract" xml:lang="en">Efficient assembly of 6‐substituted 4‐aryl‐5‐oxo‐1,4,5,7‐tetrahydropyrrolo[3,4‐b]pyridines (7a‐f) is described according to a Hantzsch type reaction from formyl‐ester 4 by imination, borohydride reduction and intramolecular thermal amino‐ester cyclization. The starting compound 4 was prepared in three steps from the readily available formyl derivative 1, methyl 4,4‐dimethoxy‐3‐oxobutanoate and methyl 3‐aminocrotonate.</div>
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Facile access to 6‐substituted 1,4,5,7‐tetrahydropyrrolo[3,4‐b]‐pyridines via hantzsch type dimethyl 4‐aryl‐2‐formyl‐6‐methyl‐1,4‐dihydropyridine‐3,5‐dicarboxylates

Facile access to 6‐substituted 1,4,5,7‐tetrahydropyrrolo[3,4‐b]‐pyridines via hantzsch type dimethyl 4‐aryl‐2‐formyl‐6‐methyl‐1,4‐dihydropyridine‐3,5‐dicarboxylates

Source :

Abstract

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